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where the terms are as in Eq. 3.33, c D the speed of light (2.998 1010 cms 1 ), and A is the measured hyper ne coupling for the units shown as subscripts. For example, a measured A value of 56 gauss at g D 1.97 is 51.5 10 4 cm 1 whereas a 56-gauss coupling at the free electron value (g D 2.0023) is 52.4 10 4 cm 1 . Both round to 52 10 4 cm 1 . Rounding is appropriate because most results are imprecise by 3 10 4 cm 1 units or more. However, at g D 2.20 [an average g value for many copper(II) compounds] a 56-gauss coupling is 58 10 4 cm 1 , and iron(III) species often have average g values >4, where a 56-gauss coupling would have an energy of >100 10 4 cm 1 . Irradiated organic polymers are predominantly split by the hydrogen nuclei (protons, I D 1/2) in the radicals. The number of peaks gets quite large because nuclei in difference symmetry create separate sets. A methylene (CH2 ) group on a radical has three resonances from the two equivalent protons interacting with the electron (2nH IH C 1 D 3), whereas a radical with two nonequivalent CH2 groups provides nine resonances (the product of 3 for one CH2 times 3 for the second one). This is shown schematically in Figure 3.33. When transition metal ions with large I and A values are involved in radicals, the details of the organic portion are often washed out. However, in simpler cases the EPR spectra show both the metal and nonmetal spin interactions although even in monomers not all of the anticipated lines are observed. Figure 3.34 shows an EPR spectrum for bis(salicylaldiminato)copper(II), a model monomer excel barcode add in free download Barcode Add-in for Excel for Mac - Free download and software ...
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